Application Type
Patents
Application SubType
PCT
(10) Registration Number and Date
Status
Filed-Accordance of filing date
(180) Expiration Date
(20) Filing Number and Date
PG P/2024/000039 2023.07.26
(40) Publication Number and Date
(86) PCT Filing Number and Date
(87) PCT Publication Number and Date
(85) National Entry Date
(30) Priority Details
(51) IPC Classes
(72) Inventor
(74) Representative Name
(EN) VAI IP COMMERCIAL : P.O BOX 27, KONEDOBU, NATIONAL CAPITAL DISTRICT
(54) Title
(EN) METHOD FOR PREPARING BATTERY-GRADE NICKEL-COBALT-MANGANESE SULFATE SOLUTION FROM LOW NICKEL MATTE
(57) Abstract
(EN)

The disclosure discloses a method for preparing a battery-grade nickel-cobalt-manganese sulfate solution from low nickel matte. The method includes the following steps: grinding low nickel matte, then adding the ground low nickel matte to concentrated sulfuric acid, and carrying out atmospheric pressure leaching to obtain a first slag phase and a first liquid phase; carrying out evaporation concentration-cooling crystallization on the first liquid phase to obtain ferrous sulfate crystals; adding concentrated sulfuric acid to the first slag phase, and carrying out oxygen pressure leaching to obtain a second slag phase and a second liquid phase; adjusting pH of the second liquid phase to 3-4 to generate a precipitate, and removing the precipitate by filtration to obtain a filtrate; carrying out adsorption treatment on the filtrate by adopting chelating resin; washing the adsorbed chelating resin with a first sulfuric acid solution to obtain a washing solution containing Mg and Mn, and then washing the chelating resin with a second sulfuric acid solution to obtain a nickel-cobalt sulfate solution; and mixing the nickel-cobalt sulfate solution with the washing solution containing Mg and Mn to obtain the nickel-cobalt-manganese sulfate solution. According to the method of the disclosure, the battery-grade nickel-cobalt sulfate solution is prepared from the low nickel matte as a raw material, so that the recovery rate of nickel and cobalt is increased, and the acid consumption is reduced.

(58) Citations
Document Type Date Action
Event NameDateStatus
Filing2023.07.26Filed
PCT National Phase Entry2023.07.26PCT National Phase
Filing2025.01.16Filed